3-(4-Hydroxyphenyl)-1-propanol | CAS:10210-17-0

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Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to 24 months(2-8C).

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Synthesis of (-)-Monoterpenylmagnolol (XI) and Magnolol (XII).[Reference: WebLink]

METHODS AND RESULTS:
(-)-Monoterpenylmagnolol (3) was synthesized in eight steps from (+)-3,9-dibromocamphor (4) and the bis(methoxymethyl) ether (22) of 3-(4-Hydroxyphenyl)-1-propanol. Fragmentation of an endo-3-aryl-9-bromocamphor (27) provided the correct absolute stereochemistry. In this total synthesis, dissolving metal conditions were developed to reduce enol phosphate and isopropenyl functions without concomitant reduction of an attached phenol. Palladium(O)-catalyzed cross-coupling of an arylzinc chloride with 4-allyl-2-iodophenyl methoxymethyl ether (34) provided the desired tricyclic 1,2,3,5-tetrasubstituted biaryl 41 in fair yield without optimization and with little isomerization of the allyl group.
CONCLUSIONS:
Magnolol (1) was also synthesized by aryl coupling of 34 and the methoxymethyl ether of 4-allyl-2-lithiophenol via the zinc chloride method as above, as well as from 5,5'-dibromo-2,2'-dimethoxybiphenyl (37) by allylation with allyltributylstannane followed by ether cleavage.

Product Name	3-(4-Hydroxyphenyl)-1-propanol
CAS No.:	10210-17-0
Catalog No.:	CFN99037
Molecular Formula:	C₉H₁₂O₂
Molecular Weight:	152.2 g/mol
Purity:	>=98%
Type of Compound:	Phenylpropanoids
Physical Desc.:	Oil
Source:	The fruits of Zanthoxylum cuspidatum
Solvent:	Chloroform, Dichloromethane, Ethyl Acetate, DMSO, Acetone, etc.
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