1-Indanamine
Reference standards.
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Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to
24 months(2-8C).
Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour.
Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com
The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.
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Tetrahedron, 1970, 26(1):107-118.
Optically active amines—X: Optical rotatory dispersion and circular dichroism of the N-salicylidene derivatives of α- and β-phenylalkylamines—the absolute configurations of some phenylnorbornanes.[Reference:
WebLink]
ORD and CD measurements are reported for the N-salicylidene derivatives of a number of α and β-phenylalkylamines.
METHODS AND RESULTS:
The strong positive Cotton effects near 255 and 315 nm shown by the derivatives of(S)-1-Indanamine and (1S,2S)-2,3-diphenyl-1-methylpropylamine are in accord with a planar sector rule for the prediction of the sign of the Cotton effects associated with a particular enantiomer of the N-salicylidene derivative of an α-or β-phenylalkylamine. Application of this sector rule to the interpretation of ORD and CD of the N-salicylidene derivatives of (+) exo-3-phenyl-endo-2-norbornanamine hydrochloride and (—)-endo-3-phenyl-endo-2-norbornanamine hydrochloride fixes their absolute configurations as (2S) and (2R), respectively. A tentative reassignment of the (S) configuration is made to (+)-1,2,2-triphenylethylaminehydrochloride on.
