Asperumine
Reference standards.
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Providing storage is as stated on the product vial and the vial is kept tightly sealed, the product can be stored for up to
24 months(2-8C).
Wherever possible, you should prepare and use solutions on the same day. However, if you need to make up stock solutions in advance, we recommend that you store the solution as aliquots in tightly sealed vials at -20C. Generally, these will be useable for up to two weeks. Before use, and prior to opening the vial we recommend that you allow your product to equilibrate to room temperature for at least 1 hour.
Need more advice on solubility, usage and handling? Please email to: service@chemfaces.com
The packaging of the product may have turned upside down during transportation, resulting in the natural compounds adhering to the neck or cap of the vial. take the vial out of its packaging and gently shake to let the compounds fall to the bottom of the vial. for liquid products, centrifuge at 200-500 RPM to gather the liquid at the bottom of the vial. try to avoid loss or contamination during handling.
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Chemistry of Natural Compounds,1974,10,(4): 483-485.
Refinement of the structure of asperumine[Reference:
WebLink]
Asperumine has been isolated from the combined alkaloids ofSymphytum caucasicum.
METHODS AND RESULTS:
The hydrolysis and hydrogenolysis of Asperumine has given heliotridine, acetone, and angelic and asperuminic acids. The structure of Asperumine has been refined on the basis of the products of hydrolysis and hydrogenolysis and also of features of the mass and NMR spectra.
CONCLUSIONS:
It has been established that Asperumine is an isomer of heliosupine in the 2,3,4-trihydroxy-2-methylpentane-3-carboxylic acid moiety.
